六 味 地 黄 丸.ppt

六味地黄丸
Liuweidihuangwan
Ingredients——处方
Procedure——制法
Description——性状
Identification——鉴别
Other requirements——检查
Assay——含量测定
Action——功能
Indication——主治
Usage and dosage——用法与用量
Specification——规格
Storage——贮藏
熟地黄
160g
山茱萸
80g
处方
(成分)
牡丹皮
60 g
山药
80g
茯苓
60 g
泽泻
60 g
pulverize: 研磨
sift:评审,过筛
Procedure/制法
以上六味,粉碎成细粉,过筛,混匀。每100g粉末加炼蜜35~50g与适量的水,泛丸,干燥,制成水蜜丸;或加炼蜜80~110g制成小蜜丸或大蜜丸,即得。
make pills : 泛丸
Description
本品为棕黑色的水蜜丸、黑褐色的小蜜丸或大蜜丸;味甜而酸。
Identification
Microscopical
Starch granules triangular-ovoid or oblong, 24~40μm in diameter, hila short cleft or V-shaped.
Irregular branched masses color less, dissolved in chloral hydrate solution: hyphae colorless, 4~6μm in diameter.
cleft:裂缝 hyphae:菌丝
chloral hydrate solution 水合***醛溶液
Epidermal cells of pericarp orange-yellow, polygonal in surface view, with somewhat beaded anticlinal walls.
epidermal: 表皮的 pericarp: 果皮
beaded anticlinal walls:垂周壁念珠状增厚
anticlinal walls of the endodermis cells sinuous, thickened, lignified, with slender pit-canals.
内皮层细胞垂周壁波状弯曲,较厚,木化,有细长孔沟。
Pulverize 6 g of the water-honeyed pills, or triturate 9 g of the small honeyed pills or big honeyed pills with 4 g of kieselguhr and triturate well.
Heat under reflux with 40 ml of ether at a low temperature for 1 hour, cool , filter and evaporate to remove ether.
kieselguhr: 硅藻土 triturate: 研匀
Physical and Chemical identification
paeonol: 丹皮酚 cyclohexane: 环己烷
ferric chloride:三***化铁 hydrochloric acid :盐酸
5% ferric chloride in ethanol acidified with hydrochloric acid
盐酸酸化的5%三***化铁乙醇溶液
供试品色谱中,在与对照品色谱相应的位置上显相同的蓝褐色斑点。