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n n’二水杨酰基苯二甲酰二肼和取代脲的合成及应用.docx


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目 录
第 1 章文献综述····················································································· 1
酰肼类及取代脲类化合物的用途························································· 1
酰肼类化合物的用途··································································· 1
取代脲类化合物的用途································································ 3
酰肼类及脲类化合物文献合成方法······················································ 4
酰肼类化合物文献的合成方法······················································ 4
取代脲类化合物的文献合成方法··················································· 6
酰肼类及脲类化合物文献合成方法的评述············································· 9
酰肼类化合物文献合成方法的评述················································ 9
脲类化合物文献合成方法的评述··················································· 9
本论文的研究目的和意义································································ 9
第2 章实验部分····················································································11 实验仪器和试剂·············································································11
实验仪器·················································································11
主要实验试剂···········································································11
N,N’-二水杨酰基-1,3(1,4)-苯二甲酰二肼及中间体的合成 12
水杨酸苯酯(3)的合成·································································12
水杨酰肼(4)的合成与苯酚的回收··················································12
间苯二甲酰氯(5)的合成······························································13
间苯二甲酸二甲酯的合成···························································13
间苯二甲酸二酰肼(9)的合成························································13
水杨酰氯(10)的合成···································································13
N,N’-二水杨酰基-1,3-苯二甲酰二肼(7)的合成 13
对苯二甲酰氯(6)的合成······························································14
N,N’-二水杨酰基-1,4-苯二甲酰二肼(8)的合成 14
单取代脲类化合物的合成·································

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